Effect of Aging Procedures on Phase Transformation of Posterior 3-Unit Zirconia Frameworks Used in Fixed Partial Dentures


BÜLBÜL M., Palta N., ERDİNÇ G.

Nigerian Journal of Clinical Practice, cilt.28, sa.2, ss.188-194, 2025 (SCI-Expanded) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 28 Sayı: 2
  • Basım Tarihi: 2025
  • Doi Numarası: 10.4103/njcp.njcp_579_23
  • Dergi Adı: Nigerian Journal of Clinical Practice
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus, MEDLINE
  • Sayfa Sayıları: ss.188-194
  • Anahtar Kelimeler: Aging, phase transformation, XRD, Y‑TZP, Zirconia
  • Bilecik Şeyh Edebali Üniversitesi Adresli: Evet

Özet

Background: Zirconia is an essential material for dentistry, and its properties should be investigated in all aspects. Aim: The primary objective of this study was to assess the impact of aging procedures on the phase transformation of posterior 3-unit zirconia frameworks used in fixed partial dentures. Setting and Designs: The study considered three aging procedures: Group T underwent thermocycling with 20,000 cycles between 5°C and 55°C for 30 seconds, Group M experienced mastication cycles with 500,000 cycles at 1.3 Hz and 49 N force, and Group T + M was subjected to consecutive thermocycling (20,000 cycles/5–55°C/30 s) and mastication cycles (500,000 cycles/1.3 Hz/49 N). Methods: E ach group comprised 12 specimens from manufactured presintered zirconia blocks (inCoris ZI, Sirona, Salzburg, Austria). The evaluation of phase transformation was performed through X-ray diffraction (XRD) analysis. Statistical Analysis: The obtained data were subjected to statistical analysis using one-way ANOVA and the Tukey tests (α = 0.05). Results: The study revealed statistically significant differences in the effects of aging processes on phase transformation in zirconia frameworks (P < 0.05). Group T + M demonstrated the highest phase transformation compared to other groups (P < 0.05). Moreover, significant differences were observed between the distal connector and pontic regions (P < 0.05). Conclusion: All aging processes applied to zirconia increased the amount of monoclinic phase.